ASM vol.1 no.73 from June 1969, written by Stan Lee with cover art from John Romita, and just as Silvermane and the Maggia find out that the Shocker has left the Lifeline Tablet in his girlfriend care, and send Man Mountain Marko to obtain it, Capt Stacy informs Spider-Man that his info leads to the same place! So naturally, Man Mountain Marko & Spidey face off against each other for the very first time! The fight doesn't last very long, as Marko throws the Shocker's girl out the window, forcing Spider-Man to save her life while Marko makes off with the tablet! Back at Silvermane's place, we see Dr. Curt Connors, who has been kidnapped to assist with translating the tablet, warning that he should not be kept prisoner because it's dangerous, but refuses to elaborate!
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